No 1 (2021)

Full Issue

Regulation of powder particles shape and size at plasma spraying

Ermakov S.B.

Abstract

Additive technologies are among the most rapidly developing areas of modern production. To ensure the progressive movement of additive technologies development in the Russian Federation, it is necessary to provide maximum availability of additive raw materials – spherical metal powders for the domestic enterprises; however, the absence of domestic assemblies to produce such powders hampers the solution of this issue. Peter the Great St. Petersburg Polytechnic University has developed and successfully carried out industrial tests of a plasma atomization system for solid metal feedstocks of various chemical compositions. The paper presents the results of the study of the influence of some technological parameters on the granulometric size, shape, and defect structure of 12H18N9 steel and VG98 alloy powders. The paper includes the results of the research of the influence of such spraying parameters as the current strength and the plasma-forming gas velocity supplied to the plasma generator and the volume of protective gas supplied to the spray torch through the fluidized bed system nozzles located in the midsection of the atomizer spraying chamber. The study showed that by increasing the current strength and the plasma-forming gas velocity, it is possible to reduce the average size of the powder particles; and by changing the volume of the protective gas supply, it is possible to control the particle shape. The analysis of the chemical composition of the obtained powders shows that during the spraying process, there is no loss of alloying elements and the powder composition is the same as the original feedstock compositions. The paper gives the developed modes for the alloy feedstocks spraying, shows the possibility to produce metal powders with the level of the spherical shape factor of 92–96 % and minimal – not exceeding 0.5 % of powder aggregate weight – number of particles with nonmetallic inclusions, external and internal defects.

Frontier Materials & Technologies. 2021;(1):7-15
pages 7-15 views

Structural phase transformations during deformation Of Fe-Co-V alloys using the high-pressure torsion method

Muradimova L.F., Glezer A.M., Shirshikov S.O., Shchetinin I.V., Dyakonov D.L.

Abstract

Fe-Co alloys belong to the soft magnetic materials and have an extremely high value of saturation magnetization σ at room temperature. In particular, Fe-Co alloy with the equiatomic ratio of components at room temperature has the maximal σ value among all known ferromagnetic materials. Unfortunately, it is hard to reproduce the unique magnetic properties of these alloys (especially Fe-Co alloys) due to their high fragility caused mainly by the formation of far atomic ordering according to B2 type in the structure. Adding vanadium to the Fe-Co alloys increases plasticity, but it reduces basic magnetic characteristics. In this paper, using the X-ray structural analysis, transmission scanning microscopy, and magnetometry, the authors analyzed the influence of high-pressure torsion at the temperatures of 77 and 295 K on the structure and phase composition of soft magnetic alloys (Fe-Co)100-xVx (x=0–6.0). As the principal structural parameter before and after deformation, the authors analyzed the magnitude of γ-phase volume ratio in the BCC magnetic matrix. The study identified that plastic deformation causes the suppression of formation of excessive γ-phase in alloys containing (3.0–6.0) % V. The study shows that the loss of γ-phase is observed with the increase of high-pressure torsion deformation firstly in the alloys with the high vanadium proportion and at the deformation effect at higher temperature (295 K). The authors conclude that the detected effect is a consequence of γ→α martensite transformation caused by deformation by analogy to TRIP-effect. The study identified that the suppression of paramagnetic γ-phase leads to a noticeable increase in the specific saturation magnetization.

Frontier Materials & Technologies. 2021;(1):16-23
pages 16-23 views

Estimation of texture parameters for the precision surfaces using the quasioptimal correlation algorithms

Nоsоv N.V., Kоstin N.A., Ladyagin R.V.

Abstract

The authors considered a new method of texture analysis of machined precision surfaces based on using computer optics and the autocorrelation method of processing the images of micro-relief textures under the study. This method is based on a probabilistic comparative evaluation of the unknown texture of the micro-relief under the investigation with the available textures of reference micro-patterns, in which microrelief parameters are determined. The paper proposes an approach to identify the profile surface roughness of a gas turbine engine (GTE) blade after vibro-contact polishing according to the parameters of correlation surface texture. The authors studied the surface micro-geometry of the blade back and pressure side using the optoelectronic complex based on the calculation of the average amplitude of the variable component of an autocorrelation function resulting from computer processing of a surface video image. The application of the electrooptic method for evaluating the surface texture of compressor and turbine blades allows building the surface roughness fields and more deeply analyzing the technology of final processing of the GTE blade feather profile. The relevance and novelty of the study lie in the promising technique to evaluate the surface quality parameters using the electrooptic method. A special feature of this method is the measurement of surface area roughness, while the stylus methods measure the roughness of the surface profile. An important advantage of the proposed method is its application to measure the roughness parameters of a curved surface by a non-contact method, which is advanced since there are surfaces of parts that do not imply being scratched with a diamond needle.

Frontier Materials & Technologies. 2021;(1):24-31
pages 24-31 views

Development of turning process digital twin based on machine learning

Rastorguev D.A., Sevastyanov A.A.

Abstract

Today, manufacturing technologies are developing within the Industry 4.0 concept, which is the information technologies introduction in manufacturing. One of the most promising digital technologies finding more and more application in manufacturing is a digital twin. A digital twin is an ensemble of mathematical models of technological process, which exchanges information with its physical prototype in real-time. The paper considers an example of the formation of several interconnected predictive modules, which are a part of the structure of the turning process digital twin and designed to predict the quality of processing, the chip formation nature, and the cutting force.  The authors carried out a three-factor experiment on the hard turning of 105WCr6 steel hardened to 55 HRC. Used an example of the conducted experiment, the authors described the process of development of the digital twin diagnostic module based on artificial neural networks. When developing a mathematical model for predicting and diagnosing the cutting process, the authors revealed higher accuracy, adaptability, and versatility of artificial neural networks. The developed mathematical model of online diagnostics of the cutting process for determining the surface quality and chip type during processing uses the actual value of the cutting depth determined indirectly by the force load on the drive. In this case, the model uses only the signals of the sensors included in the diagnostic subsystem on the CNC machine. As an informative feature reflecting the force load on the machine’s main motion drive, the authors selected the value of the energy of the current signal of the spindle drive motor. The study identified that the development of a digital twin is possible due to the development of additional modules predicting the accuracy of dimensions, geometric profile, tool wear.

Frontier Materials & Technologies. 2021;(1):32-41
pages 32-41 views

Use of digital twins for mathematical modeling of ultrasonic drilling of titanium blanks

Savelyev K.S., Ilyushkin M.V., Kiselev E.S.

Abstract

The paper considers the creation and research of a virtual prototype of titanium blanks drilling using the Lagrange and Galerkin method. The developed finite-element models are designed to study the process of mechanical treatment and optimize technological cutting parameters. The paper presents the results of computational investigation of titanium blanks drilling using mathematical modeling programs, which allow complete simulating operating procedures in a computer (digital twin). As a program to simulate the process of removing the allowance from a titanium workpiece, the authors used a multipurpose software product of finite-element modeling and analysis of highly-linear dynamic processes using various Ls-DYNA time integration schemes. The application of the Galerkin method allows adequately describing the drilling process with the introduction of the ultrasonic field energy into a treatment zone, can significantly reduce the duration of experimental research and evaluates the influence of the cutting mode elements and the tool design parameters on the power and energy aspects of the formation of new machine parts surfaces. Both methods are applicable to create various processes of mechanical treatment, however, the Lagrange method is less sensitive to the ultrasonic field energy. The introduction of the ultrasonic field energy into the drilling zone of workpieces made of hard-processing titanium alloys can significantly reduce energy costs. As a result of the simulation, the authors obtained a calculation file containing the simulation process, the solution of which visually reflects the drilling process of a titanium workpiece in a real-life setting with the removal of chips. However, for complete verification of numerical study results, it is necessary to carry out an experimental check and make adjustments to the calculated data.

Frontier Materials & Technologies. 2021;(1):42-54
pages 42-54 views

The enhancement of cutting capacity of a grinding wheel when processing ductile steel blank parts by ultrasonic activation

Khazov A.V., Unyanin A.N.

Abstract

The study aimed to identify the relations between the sticking intensity and ultrasonic vibrations (UV) used for processing and evaluate the wheels’ performance when grinding ductile materials blank parts. The authors carried out the numerical simulation of local temperatures and the 3H3M3F steel workpiece temperature when grinding by ultrasonic activation. The study determined that the application of ultrasonic vibrations with the amplitude of 3 µm causes the decrease in local temperatures by 13…40 %, and in blank part temperature – up to 20 %. The calculation identified that the activation of ultrasonic vibrations with the amplitude of 3 µm causes the decrease in the glazing coefficient by 33 % for cutting grain and by 7 % for deforming grain. When increasing the longitudinal feed rate or the grinding depth, the glazing coefficient increases to a lesser degree when using the ultrasonic vibration than in the case without ultrasonic activation. The authors carried out the numerical simulation of local temperatures when scratching the 3H3M3F steel specimens by single abrasive grains with ultrasonic activation. The sticking deformation and the stresses resulted from this deformation and affecting the junction points of sticking with grains with and without ultrasonic vibrations application are calculated. The experimental research included the micro-cutting of specimens with single abrasive grains. The experiments identified that the abrasive grains wear out and glaze to a lesser degree when micro-cutting a workpiece with ultrasonic vibrations activation. The lowering of the intensity of sticking of the workpiece material particles to the abrasive grains due to the adhesion causes the decrease in the glazing coefficient when using ultrasonic activation. The study considered the possibility to enhance the efficiency of flat grinding through the use of the energy of ultrasonic vibrations applied to a blank part in the direction with the grinding wheel axis. A workpiece fixed in the device between the vibration transducer and the support is one of the components of a vibration system. The authors performed the experiment when grinding 3H3M3F and 12H18N10T steel workpieces with the wheel face. When grinding with ultrasonic vibrations, the grinding coefficient increases up to 70 %, and the redress life increases twice or thrice.

Frontier Materials & Technologies. 2021;(1):55-62
pages 55-62 views

The comparative analysis of thermal effects in elastomers modified with MCNT at constant DC voltage

Shchegolkov A.V.

Abstract

The author carried out the comparative analysis of elastomers – polyurethane (NPC) and silicone compound (NCOC) modified with carbon nanotubes (MCNT) with a mass content of 1 to 9 %. MCNTs were synthetically produced by the CVD technology using Co-Mo/Al2O3-MgO (MCNT1) and Fe-Co/2,1Al2O3 (MCNT2) catalysts. The analysis of experimental study results showed that the lowest specific bulk electrical conductivity (5×10-10 Cm×cm-1) was typical for polyurethane elastomer (1 mass. % MCNT synthetically produced using Fe-Co/2,1Al2O3 catalyst). For the silicone elastomer modified with 9 mass. % MCNT1, the specific bulk electrical conductivity was 4×10-1 Cm×cm-1. The author identified the parameters of percolation of electrical conductivity model for NPC, NCOC with MCNT1 and MCNT2, taking into account the MCNT packing factor and electrical conductivity critical index. The maximum temperature field uniformity is typical for silicone elastomer with 7 mass. % MCNT2. Nonuniform temperature field in modified polyurethane-based elastomers can be caused by the local MCNT entanglement manifested in the creation of agglomerates or more dense electrically-conductive circuit packing, which, in its turn, results in the decrease in heat power. The heating temperature of nanomodified composites produced from NCOC 1 and NCOC 2 can vary from 32.9 to 102 °С. The author studied the modes of nanomodified elastomers heat generation in the range of 6 to 30 V, compared heat generation in the elastomer-based and ceramics-based samples. The study allowed identifying the best combination of the polymeric matrix and MCNT type. For the electric heater, it is the most efficient to apply silicone compound at the 7 % MCNT concentration and, depending on the feeding voltage level of 12 or 24 V, to use MCNT1 or MCNT2.

Frontier Materials & Technologies. 2021;(1):63-73
pages 63-73 views

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